1. Carpino, LA and others., Org. Synth., 44, 15, 1964. 2. Sakai, K. and others., J. Org. Chem., 36, 2387, 1971. 3. Fenlon, W.J., Chem. News of the Engineer, 54, 3, 1976. 4. Koppel, H.C., Chem. News of the Engineer, 54, 5, 1976. 5. Aldrich Advertizement, J. Chem. Soc. Chem. Commun., 23, I, 1976. 6. Feyen, P., Angew. Chem. (Int. Editor), 16, 115, 1977. 7. F and F 1, 84, 2, 44, 3, 36, 4, 54, 6, 77. 8. Armour, MA, Chemical processing methods {treatment} {minimize waste waste}, in preventing pollution and Waste Minimization in Laboratories, Reinhardt, PA and others., editors. Lewis Publishers, Boca Raton, FL, 1995, p. 282. AZ of chemical names {Name} 109 tert-butyl HYDROPEROXIDE (CH3) 3COOH FIRE HAZARD Physical Properties Colourless liquid; stable below 75 ° C; MP, -8 ? C.1 Fire Danger Fire {} Item {Point} outbreak, 27 ° C. Extinguish the fire} {fire with water spray aerosol, {}, dry chemical, carbon dioxide, or evaporation liquids.2 Chemical Properties Slightly soluble soluble {} in water3; very soluble in} {soluble esters and alcohols.4 Hazardous Reactions May explode when distilled 5.6 Physiological Properties and Health Hazards The liquid irritates the eyes and skin. Poisonous if ingested. Avoid contact with skin, eyes and clothing 3 Instruction Break Wear eye protection, lab coat, and nitrile rubber gloves. Work due to the body {body} shield. Shedding of the coating with a 1:1:1 sulphuric acid mixture by weight of sodium carbonate or calcium carbonate, clay cat litter (bentonite), and sand. Carefully select a beaker using a plastic scoop. Follow the procedure is unnecessary seven orders Moet spill area thoroughly with soap and water. Waste Disposal Wear nitrile rubber gloves, eye protection and lab coat. Work hard from behind Shield body {body} in the hood smoke. Carefully add the peroxide to a 10% aqueous sodium bisulfite th Hazardous laboratory chemicals disposal of lead 110 (Peroxide to 10 ml / g). Continue to stir for 24 hours. Ending with a decision can be washed a leak in August Reaction to breaking and Waste Orders LINKS {Recommendations} 1. Merck 1569. 2. NFPA 325M. 3. Suite 261. 4. Saxophone {hammer} 447. 5. Milas, N.A. and others., J.. Chem. Soc., 68, 205, 1946. 6. B 488. 7. Armour, MA, Brown, LM, and Plotinus, GL, J. Chem. Education, 62, A93, 1985. 8. PPL 170. AZ of chemical names {Name} 111 tert-butyl HYPOCHLORITE (CH3) 3COCl WAREHOUSE STORE {} in the refrigerator DARK Physical Properties Pale yellow liquid with irritation flavor; base point, 77-78 ° C.1 Hazardous Reactions Ampoules are prone to explosion ripped {} if not stocked {} is not stored in a cool, dark place. This should not be heated above his point {dot} 2, 3, boiling a severe reaction if exposed to {} subjected to strong light or an overheating Rubber. Strong reaction 3 Physiological properties and health hazards: Vapor irritates the mucous membranes and eyes. Wear eye protection, lab coat, and nitrile rubber gloves. Work hard from behind Shield body {body}. Shedding of the coating with a 1:1:1 mixture by weight of sodium carbonate or calcium carbonate, clay cat litter (bentonite), and sand. Carefully scoop out the mixture into a beaker cold water in the hood smoke. Add 10% solution of sodium bisulfite, allowing 10 ml bisulfite solution to each 1 ml of spilled hypochlorite. Let stand until the body does not settle. Filter the liquid into the drain. The solid residue can be discarded as a normal failure 4 Wash spill area thoroughly with soap and water. Waste Disposal Wear nitrile rubber gloves, laboratory coats and eye protection. Work in the hood smoke. Slowly add the t-butyl hypochlorite to an excess of stirred, cold steel of a 10% solution sodium bisulfite. Allow 10 ml bisulfite solution to each 1 ml of hypochlorite. When the reaction is stopped, taking a leak in March t-butyl hypochlorite and decomposes with UV light 2,3,5 LINKS {Recommendations} 1. Merck 1570.